CJFST.2026.18.1.10

Moisture desorption isotherms and drying kinetics of pasta enriched with pecan nut flour

https://orcid.org/0000-0001-8142-3459 Gabriela Silvina Muchiutti1, https://orcid.org/0000-0003-3345-4212 Nancy Genoveva Cámera1, https://orcid.org/0000-0002-1220-5834Virginia Judit Larrosa1,2*

1University National of Entre Ríos, Faculty of Bromatology, President Perón 1154 St. Educational Pole, Gualeguaychú, 2820, Entre Ríos, Argentina
2Institute of Food Science and Technology of Entre Ríos (ICTAER), President Perón 1154 St., Gualeguaychú, 2820, Entre Rios, Argentina

ARTICLE INFO ABSTRACT
TYPE: Original scientific paper
https://doi.org/10.17508/CJFST.2026.18.1.10
PDF
The growing interest in nutritionally enhanced pasta products has driven the search for functional ingredients capable of improving their lipid, protein, and fibre profiles. Pecan nut flour, a by-product of the oil extraction industry, represents a promising alternative; however, its incorporation into pasta formulations modifies dough physicochemical properties and requires optimisation of the drying process to ensure product stability. This study characterised moisture desorption isotherms and drying kinetics of noodles formulated with a 1:1 wheat flour–pecan nut flour ratio. Isotherms were determined at 25 °C and 40 °C (aw: 0.20–0.92) and fitted to GAB and Oswin models. Drying was performed at 30 °C and 50 °C with 40% relative humidity. The GAB model showed the best fit (R² = 0.99; E% < 5%) with monolayer moisture contents of 0.188 and 0.0996 g water/g dry matter at 25 °C and 40 °C, respectively. Drying kinetics were dominated by the falling rate period, described by Fick’s second law, yielding diffusion coefficients of 6.62 × 10⁻¹² m²/s (30 °C) and 1.80 × 10⁻¹¹ m²/s
(50 °C). Both conditions produced final moisture contents and water activity values complying with Argentine Food Code limits and microbiological stability thresholds, confirming the technological feasibility of pecan nut flour as a functional ingredient in dry pasta production.
*CORRESPONDENCE
Virginia Judit Larrosa
virginia.larrosa@uner.edu.ar
ARTICLE HISTORY
Received: April 1, 2026
Accepted: June 24, 2026
CITATION
Muchiutti GS, Genoveva Cámera N, Larrosa VJ. Moisture desorption isotherms and drying kinetics of pasta enriched with pecan nut flour. Croatian Journal of Food Science and Technology (2026) 18 (1) 134―146
COPYRIGHT: © 2026 by the author(s). This is an open-access article distributed under the terms of the Creative Commons Attribution-NonCommercial-NoDerivs (CC BY-NC-ND).
KEYWORDS

pecan nut flour; sorption isotherms; drying kinetics; effective diffusivity

KEY CONTRIBUTION

First characterisation of moisture desorption isotherms of noodles with 50% pecan nut flour. Validation of the GAB model as the best fit for predicting sorption behaviour. Determination of drying kinetics and effective moisture diffusivity at different temperatures. Demonstration of safe moisture content and water activity levels under optimised drying conditions. Contribution to the valorisation of pecan nut flour as a functional ingredient in pasta production.